{"id":17598,"date":"2018-01-24T06:08:12","date_gmt":"2018-01-23T22:08:12","guid":{"rendered":"\/\/www.gsbet888.com\/?p=17598"},"modified":"2019-08-02T18:52:05","modified_gmt":"2019-08-02T10:52:05","slug":"%e6%af%94%e5%90%89%e5%86%85%e5%88%a9%e5%8f%8d%e5%ba%94-biginelli-reaction","status":"publish","type":"post","link":"\/\/www.gsbet888.com\/reactions\/2018\/01\/%e6%af%94%e5%90%89%e5%86%85%e5%88%a9%e5%8f%8d%e5%ba%94-biginelli-reaction.html","title":{"rendered":"\u6bd4\u5409\u5185\u5229\u53cd\u5e94 Biginelli Reaction"},"content":{"rendered":"<h4>\u6982\u8981<\/h4>\n<p>\u4e09\u7ec4\u5206\u7f29\u5408\u53cd\u5e94(Three-Component Reaction)\u4e2d\u7684\u7684\u4e00\u79cd\u3002<\/p>\n<p>\u4ea7\u7269\u4e8c\u6c22\u5627\u5576\u916e\u9aa8\u67b6\u662f\u6297\u766b\u75eb\u836f\u548c\u9499\u901a\u9053\u62ee\u6297\u5242\u4e2d\u7684\u91cd\u8981\u9aa8\u67b6\u7ed3\u6784\uff0c\u4ece\u6f5c\u5728\u610f\u4e49\u4e0a\u6765\u8bf4\uff0c\u8fd9\u662f\u4e00\u4e2a\u8fd1\u5e74\u6765\u5907\u53d7\u77a9\u76ee\u7684\u53cd\u5e94\u3002<\/p>\n<h4>\u5173\u8054\u53cd\u5e94\uff08\u672c\u7f51\u7ad9\u8bb0\u8f7d\uff09<\/h4>\n<ul class=\"list\">\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/%e5%8a%a0%e6%88%90%e5%8f%8d%e5%ba%94\/2015\/03\/%e8%b4%9d%e8%92%82%e5%8f%8d%e5%ba%94betti-reaction.html\">Betti Reaction<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/2014\/03\/%e5%85%8b%e8%84%91%e6%96%87%e7%9b%96%e5%b0%94%e7%bc%a9%e5%90%88%e5%8f%8d%e5%ba%94%ef%bc%88knoevenagel-condensation%ef%bc%89.html\">Knoevenagel-Condensation<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/2017\/03\/passerini%e5%8f%8d%e5%ba%94.html\">Passerini Reaction<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/%e7%bc%a9%e5%90%88%e5%8f%8d%e5%ba%94\/2014\/11\/bredereck%e5%98%a7%e5%95%b6%e5%90%88%e6%88%90bredereck-pyrimidine-synthesis.html\">Bredereck Pyrimidine Synthesis<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/2016\/07\/post-10081.html\">Hantzsch Dihydropyridine Synthesis<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/%e7%bc%a9%e5%90%88%e5%8f%8d%e5%ba%94\/2014\/09\/post-2825.html\">Petasis Reaction<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/%e7%bc%a9%e5%90%88%e5%8f%8d%e5%ba%94\/2014\/10\/reissert%e5%8f%8d%e5%ba%94reissert-reaction.html\">Reissert Reaction<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/2014\/05\/%e6%96%af%e7%89%b9%e9%9b%b7%e5%85%8b%e6%b0%a8%e5%9f%ba%e9%85%b8%e5%90%88%e6%88%90%e5%8f%8d%e5%ba%94-strecker-amino-acid-synthesis.html\">Strecker Amino Acid Synthesis<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/%e7%bc%a9%e5%90%88%e5%8f%8d%e5%ba%94\/2014\/07\/ugi%e5%8f%8d%e5%ba%94ugi-reaction.html\">Ugi Reaction<\/a><\/li>\n<li><a href=\"\/\/www.gsbet888.com\/reactions\/2014\/03\/%e6%9b%bc%e5%b0%bc%e5%b8%8c%e5%8f%8d%e5%ba%94-mannich-reaction.html\">Mannich Reaction<\/a><\/li>\n<\/ul>\n<h4>\u57fa\u672c\u6587\u732e<\/h4>\n<ul>\n<li>Biginelli, P. <em>Ber.<\/em> <strong>1891<\/strong>, <em>24<\/em>, 1317, DOI: <a href=\"http:\/\/dx.doi.org\/10.1002\/cber.189102401228%20\">10.1002\/cber.189102401228<\/a><\/li>\n<li>Biginelli, P. <em>Ber.<\/em><strong>1891<\/strong>, <em>24<\/em>, 2962. DOI: <a href=\"http:\/\/dx.doi.org\/10.1002\/cber.189102402126\">10.1002\/cber.189102402126<\/a><\/li>\n<li>Biginelli, P. <em>Ber.<\/em><strong>1893<\/strong>, <em>26<\/em>, 447.<\/li>\n<li>Zaugg, H. E.; Martin, W. B. <em>Org. React.<\/em><strong>1965<\/strong>,\u00a0<em>14<\/em>, 88.<\/li>\n<li>Kappe, C. O. <em>Tetrahedron<\/em><strong>1993<\/strong>, <em>49<\/em>, 6937. DOI: <a href=\"http:\/\/dx.doi.org\/10.1016\/S0040-4020%2801%2987971-0%20\">10.1016\/S0040-4020(01)87971-0<\/a><\/li>\n<li>Kappe C. O. et al. <em>Synthesis<\/em><strong>1999<\/strong>, 1799.DOI: <a href=\"http:\/\/dx.doi.org\/10.1055\/s-1999-3592%20\">10.1055\/s-1999-3592<\/a><\/li>\n<li>Lu, J.; Ma, H. <em>Synlett<\/em><strong>2000<\/strong>, 63. DOI: <a href=\"http:\/\/dx.doi.org\/10.1055\/s-2000-6469\">10.1055\/s-2000-6469<\/a><\/li>\n<li>Kappe, C. O. <em>Acc. Chem. Res.<\/em><strong>2000<\/strong>, <em>33<\/em>, 879. DOI: <a href=\"http:\/\/dx.doi.org\/10.1021\/ar000048h%20\">10.1021\/ar000048h<\/a><\/li>\n<\/ul>\n<p>&nbsp;<\/p>\n<h4>\u5f00\u53d1\u5386\u53f2<\/h4>\n<p>1891\u5e74\u7531\u610f\u5927\u5229\u5316\u5b66\u5bb6Biginelli\u9996\u6b21\u62a5\u9053\u3002<\/p>\n<div id=\"attachment_16892\" class=\"wp-caption aligncenter\">\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-17604\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2018\/01\/2014-09-07_06-29-49.png\" alt=\"\" width=\"121\" height=\"167\" \/><\/p>\n<p class=\"wp-caption-text\">Pietro Biginelli<\/p>\n<\/div>\n<h4>\u53cd\u5e94\u673a\u7406<\/h4>\n<p>\u53c2\u8003\uff1a <em><a href=\"http:\/\/dx.doi.org\/10.1021\/jo971010u\">J.\u00a0Org. Chem.<\/a><\/em><a href=\"http:\/\/dx.doi.org\/10.1021\/jo971010u\"> <strong>1997<\/strong>,\u00a0<em>62<\/em>, 7201.<\/a><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-17600 size-full\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2018\/01\/biginelli_2.gif\" alt=\"\" width=\"545\" height=\"248\" \/><\/p>\n<h4>\u53cd\u5e94\u5b9e\u4f8b<\/h4>\n<p>\u50ac\u5316\u4e0d\u5bf9\u79f0Biginelli\u53cd\u5e94\uff1a\u8fd0\u7528\u9567\u7cfb\u5143\u7d20\u590d\u5408\u7269[1]\u4e0e\u6709\u673a\u5206\u5b50\u50ac\u5316\u5242[2]\u50ac\u5316\u7684\u53cd\u5e94\u88ab\u62a5\u9053\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-17601 size-full\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2018\/01\/biginelli_3.gif\" alt=\"\" width=\"545\" height=\"106\" \/><\/p>\n<p>Batzelladine F\u7684\u5408\u6210[3]\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-17602 size-full\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2018\/01\/biginelli_4.gif\" alt=\"\" width=\"534\" height=\"147\" \/><\/p>\n<h4>\u5b9e\u9a8c\u6b65\u9aa4<\/h4>\n<p>&nbsp;<\/p>\n<h4>\u5b9e\u9a8c\u6280\u5de7<\/h4>\n<p>&nbsp;<\/p>\n<h4>\u53c2\u8003\u6587\u732e<\/h4>\n[1] Huang, Y.; Yang, F.; Zhu, C.<em>J. Am. Chem. Soc.<\/em> <strong>2005<\/strong>,\u00a0<em>127<\/em>, 16386. DOI: <a href=\"http:\/\/dx.doi.org\/10.1021\/ja056092f\">10.1021\/ja056092f<\/a>[2] Chen, X.-H.; Xu, X.-X.; Liu, H.; Cun, L.-F.; Gong, L.-Z. <em>J.\u00a0Am. Chem. Soc<\/em>. <strong>2006<\/strong>, <em>128<\/em>, 14802. DOI:\u00a0<a href=\"http:\/\/dx.doi.org\/10.1021\/ja065267y\">10.1021\/ja065267y<\/a>[3] Cohen, F.; Overman, L. E. <em>J. Am. Chem. Soc.<\/em> <strong>2001<\/strong>,\u00a0<em>123<\/em>, 10782. DOI: <a href=\"http:\/\/dx.doi.org\/10.1021\/ja017067m%20\">10.1021\/ja017067m<br \/>\n<\/a><\/p>\n<p>&nbsp;<\/p>\n<h4>\u5173\u8054\u4e66\u7c4d<\/h4>\n<div class=\"amazonjs_item amazonjs_book\">\n<div class=\"amazonjs_image\"><a class=\"amazonjs_link\" title=\"Multicomponent Reactions\" href=\"https:\/\/www.amazon.co.jp\/Multicomponent-Reactions-Jieping-Zhu\/dp\/3527308067?SubscriptionId=AKIAI6Q3RDQBU2J6P3JQ&amp;tag=chemstation-22&amp;linkCode=xm2&amp;camp=2025&amp;creative=165953&amp;creativeASIN=3527308067\" target=\"_blank\" rel=\"noopener\" data-role=\"amazonjs_product\" data-asin=\"3527308067\"><img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/images-fe.ssl-images-amazon.com\/images\/I\/51imSrK8Q9L._SL160_.jpg\" alt=\"Multicomponent Reactions\" width=\"113\" height=\"160\" \/><\/a><\/div>\n<div class=\"amazonjs_info\">\n<h4><a class=\"amazonjs_link\" title=\"Multicomponent Reactions\" href=\"https:\/\/www.amazon.co.jp\/Multicomponent-Reactions-Jieping-Zhu\/dp\/3527308067?SubscriptionId=AKIAI6Q3RDQBU2J6P3JQ&amp;tag=chemstation-22&amp;linkCode=xm2&amp;camp=2025&amp;creative=165953&amp;creativeASIN=3527308067\" target=\"_blank\" rel=\"noopener\" data-role=\"amazonjs_product\" data-asin=\"3527308067\">Multicomponent Reactions<\/a><\/h4>\n<ul>\n<li class=\"amazonjs_price\" title=\"\u4fa1\u683c\u304a\u3088\u3073\u767a\u9001\u53ef\u80fd\u6642\u671f\u306f\u8868\u793a\u3055\u308c\u305f\u65e5\u4ed8\/\u6642\u523b\u306e\u6642\u70b9\u306e\u3082\u306e\u3067\u3042\u308a\u3001\u5909\u66f4\u3055\u308c\u308b\u5834\u5408\u304c\u3042\u308a\u307e\u3059\u3002\u5546\u54c1\u306e\u8ca9\u58f2\u306b\u304a\u3044\u3066\u306f\u3001\u8cfc\u5165\u306e\u6642\u70b9\u3067 [Amazon.co.jp \u307e\u305f\u306f Javari.jp] \u306b\u8868\u793a\u3055\u308c\u3066\u3044\u308b\u4fa1\u683c\u304a\u3088\u3073\u767a\u9001\u53ef\u80fd\u6642\u671f\u306e\u60c5\u5831\u304c\u9069\u7528\u3055\u308c\u307e\u3059\u3002\"><b>\u53c2\u8003\u4fa1\u683c<\/b><span class=\"amazonjs_listprice\">\uffe5 33,707<\/span><br \/>\n<b>\u4fa1\u683c<\/b>\uffe5 33,390(2018\/01\/08 14:01\u6642\u70b9)<\/li>\n<li><b>\u51fa\u7248\u65e5<\/b>2005\/03\/04<\/li>\n<li><b>\u5546\u54c1\u30e9\u30f3\u30ad\u30f3\u30b0<\/b>1,682,932\u4f4d<\/li>\n<li><b>\u30cf\u30fc\u30c9\u30ab\u30d0\u30fc<\/b>484\u30da\u30fc\u30b8<\/li>\n<li><b>ISBN-10<\/b>3527308067<\/li>\n<li><b>ISBN-13<\/b>9783527308064<\/li>\n<li><b>\u51fa\u7248\u793e<\/b>Wiley-VCH<\/li>\n<\/ul>\n<\/div>\n<p><a class=\"amazonjs_review\" title=\"Multicomponent Reactions \u30ab\u30b9\u30bf\u30de\u30fc\u30ec\u30d3\u30e5\u30fc\" href=\"https:\/\/www.amazon.jp\/reviews\/iframe?akid=AKIAI6Q3RDQBU2J6P3JQ&amp;alinkCode=xm2&amp;asin=3527308067&amp;atag=chemstation-22&amp;exp=2018-01-09T05%3A01%3A22Z&amp;v=2&amp;sig=sBfncxEhuVaiXxjXhAYYnB3TC%252Bt62EJ96WXtOdY%252Fckk%253D&amp;TB_iframe=true&amp;height=500&amp;width=600\" target=\"_blank\" rel=\"noopener\">\u30ab\u30b9\u30bf\u30de\u30fc\u30ec\u30d3\u30e5\u30fc\u3092\u898b\u308b<\/a><\/p>\n<div class=\"amazonjs_footer\"><\/div>\n<\/div>\n<div class=\"amazonjs_item amazonjs_book\">\n<div class=\"amazonjs_image\"><a class=\"amazonjs_link\" title=\"Multicomponent Reactions in Organic Synthesis\" href=\"https:\/\/www.amazon.co.jp\/Multicomponent-Reactions-Organic-Synthesis-Jieping\/dp\/3527332375?SubscriptionId=AKIAI6Q3RDQBU2J6P3JQ&amp;tag=chemstation-22&amp;linkCode=xm2&amp;camp=2025&amp;creative=165953&amp;creativeASIN=3527332375\" target=\"_blank\" rel=\"noopener\" data-role=\"amazonjs_product\" data-asin=\"3527332375\"><img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/images-fe.ssl-images-amazon.com\/images\/I\/41J-Jn0r7wL._SL160_.jpg\" alt=\"Multicomponent Reactions in Organic Synthesis\" width=\"111\" height=\"160\" \/><\/a><\/div>\n<div class=\"amazonjs_info\">\n<h4><a class=\"amazonjs_link\" title=\"Multicomponent Reactions in Organic Synthesis\" href=\"https:\/\/www.amazon.co.jp\/Multicomponent-Reactions-Organic-Synthesis-Jieping\/dp\/3527332375?SubscriptionId=AKIAI6Q3RDQBU2J6P3JQ&amp;tag=chemstation-22&amp;linkCode=xm2&amp;camp=2025&amp;creative=165953&amp;creativeASIN=3527332375\" target=\"_blank\" rel=\"noopener\" data-role=\"amazonjs_product\" data-asin=\"3527332375\">Multicomponent Reactions in Organic Synthesis<\/a><\/h4>\n<ul>\n<li class=\"amazonjs_price\" title=\"\u4fa1\u683c\u304a\u3088\u3073\u767a\u9001\u53ef\u80fd\u6642\u671f\u306f\u8868\u793a\u3055\u308c\u305f\u65e5\u4ed8\/\u6642\u523b\u306e\u6642\u70b9\u306e\u3082\u306e\u3067\u3042\u308a\u3001\u5909\u66f4\u3055\u308c\u308b\u5834\u5408\u304c\u3042\u308a\u307e\u3059\u3002\u5546\u54c1\u306e\u8ca9\u58f2\u306b\u304a\u3044\u3066\u306f\u3001\u8cfc\u5165\u306e\u6642\u70b9\u3067 [Amazon.co.jp \u307e\u305f\u306f Javari.jp] \u306b\u8868\u793a\u3055\u308c\u3066\u3044\u308b\u4fa1\u683c\u304a\u3088\u3073\u767a\u9001\u53ef\u80fd\u6642\u671f\u306e\u60c5\u5831\u304c\u9069\u7528\u3055\u308c\u307e\u3059\u3002\"><b>\u53c2\u8003\u4fa1\u683c<\/b><span class=\"amazonjs_listprice\">\uffe5 21,607<\/span><br \/>\n<b>\u4fa1\u683c<\/b>\uffe5 21,268(2018\/01\/08 04:12\u6642\u70b9)<\/li>\n<li><b>\u51fa\u7248\u65e5<\/b>2015\/02\/09<\/li>\n<li><b>\u5546\u54c1\u30e9\u30f3\u30ad\u30f3\u30b0<\/b>404,108\u4f4d<\/li>\n<li><b>\u30cf\u30fc\u30c9\u30ab\u30d0\u30fc<\/b>512\u30da\u30fc\u30b8<\/li>\n<li><b>ISBN-10<\/b>3527332375<\/li>\n<li><b>ISBN-13<\/b>9783527332373<\/li>\n<li><b>\u51fa\u7248\u793e<\/b>Wiley-VCH<\/li>\n<\/ul>\n<\/div>\n<p><a class=\"amazonjs_review\" title=\"Multicomponent Reactions in Organic Synthesis \u30ab\u30b9\u30bf\u30de\u30fc\u30ec\u30d3\u30e5\u30fc\" href=\"https:\/\/www.amazon.jp\/reviews\/iframe?akid=AKIAI6Q3RDQBU2J6P3JQ&amp;alinkCode=xm2&amp;asin=3527332375&amp;atag=chemstation-22&amp;exp=2018-01-08T19%3A12%3A19Z&amp;v=2&amp;sig=jzeHdogvABal8sl78xWjT500t%252FSxwZChG21Zy33V2Vg%253D&amp;TB_iframe=true&amp;height=500&amp;width=600\" target=\"_blank\" rel=\"noopener\">\u30ab\u30b9\u30bf\u30de\u30fc\u30ec\u30d3\u30e5\u30fc\u3092\u898b\u308b<\/a><\/p>\n<div class=\"amazonjs_footer\"><\/div>\n<\/div>\n<h4>\u5916\u90e8\u94fe\u63a5<\/h4>\n<ul>\n<li><a href=\"http:\/\/www.organic-chemistry.org\/frames.htm?http:\/\/www.organic-chemistry.org\/namedreactions\/biginelli-reaction.shtm\">Biginelli<\/a><a href=\"http:\/\/www.organic-chemistry.org\/frames.htm?http:\/\/www.organic-chemistry.org\/namedreactions\/biginelli-reaction.shtm\">Reaction<\/a> (organic-chemistry.org)<\/li>\n<li><a href=\"http:\/\/en.wikipedia.org\/wiki\/Biginelli_reaction\">Biginelli<\/a><a href=\"http:\/\/en.wikipedia.org\/wiki\/Biginelli_reaction\">Reaction<\/a> (Wikipedia)<\/li>\n<\/ul>\n<p>&nbsp; <\/p>\n","protected":false},"excerpt":{"rendered":"\u6982\u8981 \u4e09\u7ec4\u5206\u7f29\u5408\u53cd\u5e94(Three-Component Reaction)\u4e2d\u7684\u7684\u4e00\u79cd\u3002 \u4ea7\u7269\u4e8c\u6c22\u5627\u5576\u916e\u9aa8\u67b6\u662f\u6297\u766b\u75eb\u836f\u548c\u9499\u901a\u9053\u62ee\u6297\u5242\u4e2d\u7684\u91cd\u8981\u9aa8\u67b6\u7ed3\u6784\uff0c\u4ece\u6f5c\u5728\u610f\u4e49\u4e0a\u6765\u8bf4\uff0c\u8fd9\u662f\u4e00\u4e2a\u8fd1\u5e74\u6765\u5907\u53d7\u77a9\u76ee\u7684\u53cd\u5e94\u3002 \u5173\u8054\u53cd\u5e94\uff08\u672c\u7f51\u7ad9\u8bb0\u8f7d\uff09 Betti Reaction Knoevenagel-Condensation Passerini Reaction Bredereck Pyrimidine Synthesis Hantzsch Dihydropyridine Synthesis Petasis Reaction Reissert Reaction Strecker Amino Acid Synthesis Ugi Reaction Mannich Reaction \u57fa\u672c\u6587\u732e Biginelli, P. Ber. 1891, 24, 1317, DOI: 10.1002\/cber.189102401228 Biginelli, P. Ber.1891, 24, 2962. DOI: 10.1002\/cber.189102402126 Biginelli, P. Ber.1893, 26, 447. Zaugg, H. E.; Martin, W. B. Org. React.1965,\u00a014, 88. Kappe, C. O. Tetrahedron1993, 49, 6937. DOI: 10.1016\/S0040-4020(01)87971-0 Kappe C. O. et al. Synthesis1999, 1799.DOI: 10.1055\/s-1999-3592 Lu, J.; Ma, H. Synlett2000, 63. DOI: 10.1055\/s-2000-6469 Kappe, C. O. Acc. Chem. Res.2000, 33, 879. DOI: 10.1021\/ar000048h &nbsp; \u5f00\u53d1\u5386\u53f2 1891\u5e74\u7531\u610f\u5927\u5229\u5316\u5b66\u5bb6Biginelli\u9996\u6b21\u62a5\u9053\u3002 Pietro Biginelli \u53cd\u5e94\u673a\u7406 \u53c2\u8003\uff1a J.\u00a0Org. 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