{"id":32758,"date":"2020-06-18T08:00:21","date_gmt":"2020-06-18T00:00:21","guid":{"rendered":"\/\/www.gsbet888.com\/?p=32758"},"modified":"2020-06-18T08:00:21","modified_gmt":"2020-06-18T00:00:21","slug":"%e8%89%ba%e9%ab%98%e4%ba%ba%e8%83%86%e5%a4%a7%ef%bc%8c%e9%9b%b7%e5%b0%bc%e9%92%b4%e8%bf%98%e5%8e%9f%e5%89%82%e4%b9%9f%e6%95%a2%e7%8e%a9%e7%81%ab%ef%bc%81","status":"publish","type":"post","link":"\/\/www.gsbet888.com\/%e5%8c%96%e5%ad%a6%e6%9d%82%e8%ae%b0\/recentpaper\/2020\/06\/%e8%89%ba%e9%ab%98%e4%ba%ba%e8%83%86%e5%a4%a7%ef%bc%8c%e9%9b%b7%e5%b0%bc%e9%92%b4%e8%bf%98%e5%8e%9f%e5%89%82%e4%b9%9f%e6%95%a2%e7%8e%a9%e7%81%ab%ef%bc%81.html","title":{"rendered":"\u827a\u9ad8\u4eba\u80c6\u5927\uff0c\u96f7\u5c3c\u94b4\u8fd8\u539f\u5242\u4e5f\u6562\u73a9\u706b\uff01"},"content":{"rendered":"<p>\u672c\u6587\u4f5c\u8005\uff1a\u7af9\u60a0<\/p>\n<p>\u6d77\u7ef5\u72b6\u6216\u591a\u5b54\u91d1\u5c5e\u50ac\u5316\u5242\u96f7\u5c3c\u954dRaney nickel\uff081925\u5e74\u4e13\u5229\uff09\u548c\u96f7\u5c3c\u94b4Raney cobalt\uff081933\u5e74\u4e13\u5229\uff09\uff0c\u5e7f\u6cdb\u5e94\u7528\u5728\u6750\u6599\u548c\u5927\u5b97\u5316\u5b66\u54c1\u5de5\u4e1a\u9886\u57df\u3002\u8fd9\u4e9b\u5ec9\u4ef7\u91d1\u5c5e\uff0c\u5177\u6709\u5f88\u5927\u7684\u6bd4\u8868\u9762\u79ef\uff0c\u56e0\u6b64\u6d3b\u6027\u8f83\u9ad8\uff0c\u800c\u4e14\u591a\u5b54\u7ed3\u6784\u53ef\u4ee5\u5438\u9644\u5927\u91cf\u6c22\u6c14\uff0c\u5728\u6c22\u5316\u53cd\u5e94\u4e2d\u5e94\u7528\u8f83\u591a\u3002\u5c3d\u7ba1\u6709\u79cd\u79cd\u4f18\u70b9\uff0c\u5728\u533b\u836f\u5316\u5de5\u884c\u4e1a\uff0c\u5373\u4f7f\u662f\u5c0f\u89c4\u6a21\u7684\u5b9e\u9a8c\u5ba4\u5408\u6210\uff0c\u4e5f\u5f88\u5c11\u7528\u5230\u5b83\u4eec\uff0c\u4e3b\u8981\u662f\u8fd9\u7c7b\u591a\u5b54\u6750\u6599\u4f1a\u81ea\u71c3\uff0c\u9700\u8981\u683c\u5916\u8003\u8651\u5b89\u5168\u95ee\u9898\u3002\u5373\u4f7f\u50ac\u5316\u5242\u4e3a\u72ec\u7acb\u5305\u88c5\u5bf9\u7a7a\u6c14\u7a33\u5b9a\u7684\u6d46\u72b6\u7269\uff0c\u53cd\u5e94\u7ed3\u675f\u540e\uff0c\u8fc7\u6ee4\u9664\u53bb\u50ac\u5316\u5242\uff0c\u9700\u8981\u7559\u4e00\u90e8\u5206\u6eb6\u5242\u8986\u76d6\u5728\u50ac\u5316\u5242\u8868\u9762\uff0c\u5426\u5219\u62bd\u5e72\u540e\u7684\u96f7\u5c3c\u94b4\u4f1a\u71c3\u70e7\u3002\u800c\u4e14\u6709\u673a\u5316\u5b66\u53cd\u5e94\u4e2d\u7684\u6eb6\u5242\u7edd\u5927\u90e8\u5206\u4e3a\u6709\u673a\u6eb6\u5242\uff0c\u4e5f\u662f\u4e00\u79cd\u6f5c\u5728\u7684\u71c3\u70e7\u7269\uff0c\u5373\u4f7f\u4e0d\u65ad\u5439\u60f0\u6027\u6c14\u4f53\u5982\u6c2e\u6c14\u3001\u6c29\u6c14\u4fdd\u62a4\uff0c\u4e5f\u4e0d\u80fd\u5b8c\u5168\u6d88\u9664\u9690\u60a3\u3002\u56e0\u6b64\u5373\u4f7f\u662f\u5b9e\u9a8c\u5ba4\u5c0f\u89c4\u6a21\u5b9e\u9a8c\uff0c\u4e5f\u4e0d\u80fd\u6389\u4ee5\u8f7b\u5fc3\u3002<\/p>\n<p><a href=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/1-77.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-32759 \" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/1-77.jpg\" alt=\"\" width=\"735\" height=\"260\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/1-77.jpg 1269w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/1-77-300x106.jpg 300w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/1-77-680x241.jpg 680w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/1-77-768x272.jpg 768w\" sizes=\"(max-width: 735px) 100vw, 735px\" \/><\/a><\/p>\n<p style=\"text-align: center;\">\u56fe1 \u82ef\u81481\u7684\u96f7\u5c3c\u94b4\u8fd8\u539f. \u56fe\u7247\u6765\u6e90\uff1a<em>Org. Process Res. Dev.<\/em><\/p>\n<p>\u5728\u7814\u7a76\u539f\u6599\u836f\u8fc7\u7a0b\u4e2d\uff0c\u6765\u81ea\u82f1\u56fd\u845b\u5170\u7d20\u53f2\u514bGSK\uff08GlaxoSmithKline\uff09\u7684John Jin Lim\u7b49\uff0c\u5728\u7814\u53d1\u53d6\u4ee3\u7684\u82ef\u8148<strong>1<\/strong>\u8fd8\u539f\u4e3a\u5bf9\u5e94\u7684\u82c4\u80fa<strong>2<\/strong>\u65f6\u3001\u901a\u8fc7\u7b5b\u9009\u548c\u4f18\u5316\u53cd\u5e94\u6761\u4ef6\uff0c\u96f7\u5c3c\u94b4\u662f\u7406\u60f3\u7684\u8fd8\u539f\u5242\uff0c\u53cd\u5e94\u6536\u7387\u9ad8\uff0c\u526f\u4ea7\u7269\u919b<strong>3<\/strong>\u3001\u9187<strong>4<\/strong>\u548c\u4ef2\u80fa<strong>5<\/strong>\u90fd\u8f83\u5c11\uff0c\u5982\u56fe1\u6240\u793a\u3002\u5e76\u4e14\u82c4\u80fa<strong>2<\/strong>\u4e0d\u7ecf\u7eaf\u5316\u76f4\u63a5\u8fdb\u5165\u4e0b\u4e00\u6b65\u53cd\u5e94\uff0c\u51cf\u5c11\u526f\u4ea7\u7269\u81ea\u7136\u53ef\u63d0\u9ad8\u7ec8\u4ea7\u54c1\u7684\u8d28\u91cf\u3002\u4f46\u96f7\u5c3c\u94b4\u7684\u50ac\u5316\u6548\u679c\u4f4e\u4e8e\u96f7\u5c3c\u954d\u548cPd\/C\u50ac\u5316\u5242\uff0c\u9700\u8981\u589e\u52a0\u6295\u6599\uff0c\u4f18\u5316\u540e\u7684\u7528\u91cf\u4e3a10-20 wt%\u3002\u5de5\u4e1a\u5316\u751f\u4ea7\u8be5\u4ea7\u54c1\u7684\u89c4\u6a21\u9ad8\u8fbe70-100kg\uff0c\u5178\u578b\u7684\u751f\u4ea7\u6279\u91cf\u4e3a\u4ee5100kg\u82ef\u8148<strong>1<\/strong>\u4e3a\u8d77\u59cb\u7269\u6599\uff0c\u56e0\u6b64\u9700\u898110-20kg\u7684\u96f7\u5c3c\u94b4\uff0c\u5982\u6b64\u5927\u7684\u7528\u91cf\uff0c\u5fc5\u987b\u91cd\u70b9\u8003\u8651\u5b89\u5168\u95ee\u9898\u3002GSK\u7684\u5316\u5b66\u5bb6\u53d1\u73b0\u4e86\u53ef\u4ee5\u5b89\u5168\u5904\u7406\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u7684\u6dec\u706d\u65b9\u6cd5\uff0c\u4f7f\u751f\u4ea7\u66f4\u5b89\u5168\uff0c\u8bba\u6587\u300aPlaying with Fire? A Safe and Effective Deactivation of Raney Cobalt using Aqueous Sodium Nitrate\u300b\u53d1\u8868\u5728\u5de5\u827a\u7814\u53d1\u7684\u8457\u540d\u671f\u520a<em>Org. Process Res. Dev.<\/em><em>\u4e0a\uff0c<\/em>DOI: <a href=\"https:\/\/pubs.acs.org\/doi\/abs\/10.1021\/acs.oprd.0c00053\">10.1021\/acs.oprd.0c00053<\/a>.<\/p>\n<p>\u5c3d\u7ba1\u96f7\u5c3c\u94b4\u5df2\u7ecf\u53d1\u73b0\u4e86\u8fd1\u767e\u5e74\uff0c\u5173\u4e8e\u5b83\u7684\u7814\u7a76\u62a5\u544a\u5e76\u4e0d\u591a\u3002\u53ef\u4ee5\u786e\u5b9a\u7684\u662f\u96f7\u5c3c\u94b4\u542b\u6709\u6c22\u6c14\uff0c\u867d\u7136\u6bd4\u96f7\u5c3c\u954d\u5c11\uff0c\u4e5f\u8fbe\u523040-70mlH<sub>2<\/sub>\/g\u94b4\uff0c\u5e76\u4e14\u7edd\u5927\u90e8\u5206\u6c22\u6c14\u662f\u4e0e\u94b4\u7ed3\u5408\u7684\uff0c\u901a\u8fc7\u62bd\u771f\u7a7a\u53ea\u80fd\u9664\u53bb6%\u7684\u6c22\u6c14\u3002\u96f7\u5c3c\u94b4\u5230\u5e95\u6709\u591a\u5371\u9669\uff0c\u5c1a\u672a\u6709\u7b2c\u4e00\u624b\u8d44\u6599\u3002\u5178\u578b\u7684\u5b9e\u9a8c\u5ba4\u89c4\u6a21\u7684\u6c22\u5316\u53cd\u5e94\u4e2d\uff0c\u5c061g\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u5206\u79bb\u51fa\u6765\u540e\uff0c\u5728\u73bb\u7483\u6f0f\u6597\u4e2d\u62bd\u6ee4\u5e72\u71e5\uff0c\u5e76\u76d1\u63a7\u6e29\u5ea6\u3002\u5e72\u71e5\u540e2-3\u79d2\uff0c\u7a81\u7136\u653e\u70ed\uff0c\u6e29\u5ea6\u98d9\u5347\u81f3350\u2103\uff08\u76d1\u6d4b\u5668\u7684\u6781\u9650\uff09\uff0c\u5e76\u53d1\u51fa\u70bd\u70ed\uff0c\u8bf4\u660e\u6e29\u5ea6\u81f3\u5c11\u4e3a525\u2103\uff0c\u5982\u56fe2\u6240\u793a\u3002\u5f88\u660e\u663e\uff0c\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u5177\u6709\u5371\u9669\u6027\uff0c\u5c3d\u7ba1\u6709\u62a5\u9053\u5b83\u4e0d\u5982\u96f7\u5c3c\u954d\uff0c\u6240\u4ee5\u5728\u4f7f\u7528\u96f7\u5c3c\u94b4\u65f6\u4e0d\u80fd\u62bd\u5e72\uff0c\u9700\u8981\u8986\u76d6\u4e00\u5c42\u6eb6\u5242\u6216\u6c34\u9632\u6b62\u71c3\u70e7\u3002\u5982\u679c\u627e\u4e0d\u5230\u5408\u9002\u7684\u96f7\u5c3c\u94b4\u540e\u5904\u7406\u65b9\u6cd5\uff0c\u96be\u4ee5\u83b7\u5f97\u5b89\u5168\u7684\u751f\u4ea7\u5de5\u827a\uff0c\u6240\u4ee5\u4f5c\u8005\u5fc5\u987b\u626b\u9664\u8fd9\u4e2a\u969c\u788d\u3002<\/p>\n<p><a href=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/2-75.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-32760 \" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/2-75.jpg\" alt=\"\" width=\"766\" height=\"267\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/2-75.jpg 1483w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/2-75-300x105.jpg 300w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/2-75-680x237.jpg 680w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/2-75-768x268.jpg 768w\" sizes=\"(max-width: 766px) 100vw, 766px\" \/><\/a><\/p>\n<p style=\"text-align: center;\">\u56fe2. \u76d1\u63a7\u62bd\u6ee4\u8fc7\u7a0b\u4e2d\u96f7\u5c3c\u94b4\u7684\u6e29\u5ea6\u548c\u653e\u70ed\u73b0\u8c61. \u56fe\u7247\u6765\u6e90\uff1a<em>Org. Process Res. Dev.<\/em><\/p>\n<p>\u5bf9\u6b64\uff0c\u4f5c\u8005\u8bc4\u4f30\u4e86\u4e0d\u540c\u7684\u6dec\u706d\u65b9\u6cd5\u53ca\u4f34\u751f\u7684\u5371\u9669\u3002\u5b9e\u9a8c\u5ba4\u5e38\u7528\u7684\u65b9\u6cd5\u4e3a\u52a0\u5165\u65e0\u673a\u9178\u5982\u76d0\u9178\uff0c\u4f46\u540c\u6837\u4f1a\u5267\u70c8\u653e\u70ed\u91ca\u653e\u6c22\u6c14\u3002\u800c\u4e14\u8981\u4ece\u62bd\u6ee4\u88c5\u7f6e\u4e2d\u8f6c\u79fb\u5230\u6dec\u706d\u88c5\u7f6e\u4e2d\uff0c\u8fc7\u7a0b\u540c\u6837\u6709\u5371\u9669\u3002\u4f7f\u7528\u8fc7\u7684\u6d77\u7ef5\u72b6\u50ac\u5316\u5242\u4ea7\u751f\u5316\u5b66\u5371\u9669\u7684\u6839\u6e90\u662f\u8868\u9762\u4e0a\u7684\u6d3b\u6027\u6c22\u6216\u8005\u7a7a\u4f4d\u53ef\u4ee5\u548c\u6c27\u6c14\u53cd\u5e76\u653e\u70ed\u3002\u56e0\u6b64\u4f5c\u8005\u8003\u8651\u53e6\u4e00\u79cd\u7b56\u7565\uff0c\u7528\u6c27\u5316\u5242\u5e76\u63a7\u5236\u6c27\u5316\u901f\u7387\u4ee5\u63a7\u5236\u653e\u70ed\uff0c\u5e76\u63a7\u5236\u5347\u6e29\u4e0d\u8d85\u8fc720\u2103\u3002<\/p>\n<p>\u5bf9\u4e8e\u96f7\u5c3c\u954d\uff0c\u53ef\u4ee5\u75288:1 v\/w\u76845%\u6b21\u6c2f\u9178\u94a0\u6eb6\u6db2\uff08\u6f02\u767d\u5242\uff09\u5904\u7406\uff0c\u4f46\u53ef\u80fd\u4e0d\u9002\u7528\u4e8e\u96f7\u5c3c\u94b4\uff0c\u6b21\u6c2f\u9178\u94a0NaOCl\u4f1a\u91ca\u653e\u6c27\u6c14\u5f15\u53d1\u53e6\u5916\u7684\u5371\u9669\u3002\u53d7\u52301957\u5e74\u675c\u90a6DuPont\u4e00\u7bc7\u7528\u785d\u9178\u94a0\uff08NaNO<sub>3<\/sub>\uff09\u6405\u62cc30min\u6dec\u706d\u96f7\u5c3c\u954d\u7684\u4e13\u5229\u542f\u53d1\uff0c\u4f5c\u8005\u5c1d\u8bd5\u7528\u785d\u9178\u94a0\u3001\u4e9a\u785d\u9178\u94a0\u6eb6\u6db2\u6dec\u706d\u96f7\u5c3c\u94b4\uff0c\u4f46\u4e9a\u785d\u9178\u94a0\u7684\u6548\u7387\u8f83\u5dee\u3002<\/p>\n<p style=\"text-align: center;\">\u88681. NaNO<sub>3<\/sub>\u548cNaOCl\u6dec\u706d\u7684\u653e\u70ed<\/p>\n<p><a href=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/3-61.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-32761 \" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/3-61.jpg\" alt=\"\" width=\"718\" height=\"249\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/3-61.jpg 1346w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/3-61-300x104.jpg 300w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/3-61-680x235.jpg 680w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/3-61-768x266.jpg 768w\" sizes=\"(max-width: 718px) 100vw, 718px\" \/><\/a><br \/>\n\u4e3a\u6bd4\u8f83\u4e24\u79cd\u6c27\u5316\u5242\u7684\u6dec\u706d\u6548\u679c\uff0c\u4f5c\u8005\u7528\u91cf\u70ed\u6cd5\u6bd4\u8f83NaNO<sub>3<\/sub>\u548cNaOCl\u5206\u522b\u5904\u740635g\u96f7\u5c3c\u94b4\uff08\u89c1\u5178\u578b\u6dec\u706d\u64cd\u4f5c\uff09\uff0c\u4f7f\u7528\u91cf\u4e3a20:1 v\/w\u4ee5\u5145\u5206\u6dec\u706d\u548c\u51b7\u5374\u653e\u51fa\u7684\u70ed\u91cf\u3002\u540c\u65f6\u7528CHETAH\u8ba1\u7b97\u7406\u8bba\u653e\u70ed\u91cf\u548c\u76d1\u63a7\u5b9e\u9645\u653e\u70ed\u91cf\uff0c\u4e24\u8005\u51e0\u4e4e\u4e00\u6837\uff0c\u7ed3\u679c\u89c1\u88681\u6570\u636e\u6240\u793a\u3002\u4e24\u79cd\u6c27\u5316\u5242\u90fd\u53ef\u4ee5\u6dec\u706d\u96f7\u5c3c\u94b4\uff0c\u62bd\u6ee4\u5e72\u71e5\u540e\uff0c\u5373\u4f7f\u7528\u52a0\u70ed\u677f\u5e72\u71e5\uff0c\u4e5f\u6ca1\u6709\u53d1\u73b0\u653e\u70ed\u73b0\u8c61\u3002NaNO<sub>3<\/sub>\u4f18\u52bf\u66f4\u660e\u663e\uff0c\u4f53\u7cfb\u6e29\u5ea6\u53ea\u4e0a\u5347\u4e8612\u2103\uff0c\u4f4e\u4e8e20\u2103\u7684\u9884\u671f\u5b89\u5168\u9650\u5ea6\uff0c\u800c\u4e14NaNO<sub>3<\/sub>\u4f1a\u91ca\u653e\u6c2e\u6c14\uff0cNaOCl\u91ca\u653e\u6c27\u6c14\u548c\u5c11\u91cf\u6c2e\u6c14\uff0c\u5982\u56fe3\u6240\u793a\u3002<\/p>\n<p><a href=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/4-51.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-32762 size-full\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/4-51.jpg\" alt=\"\" width=\"664\" height=\"481\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/4-51.jpg 664w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/4-51-300x217.jpg 300w\" sizes=\"(max-width: 664px) 100vw, 664px\" \/><\/a><\/p>\n<p><a href=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/5-39.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-32763 \" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/5-39.jpg\" alt=\"\" width=\"653\" height=\"435\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/5-39.jpg 720w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/5-39-300x200.jpg 300w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/5-39-680x453.jpg 680w\" sizes=\"(max-width: 653px) 100vw, 653px\" \/><\/a><\/p>\n<p style=\"text-align: center;\">\u56fe3. \u76d1\u63a7\u6dec\u706d\u8fc7\u7a0b\u4e2d\u7684\u6e29\u5ea6\u548c\u6c14\u4f53\u653e\u51fa\u60c5\u51b5\u3002\u56fe\u7247\u6765\u6e90\uff1a<em>Org. Process Res. Dev.<\/em><\/p>\n<p>\u800c\u4e14NaOCl\u548cNaNO<sub>3<\/sub>\u6dec\u706d\u96f7\u5c3c\u94b4\uff0c\u4e3b\u8981\u662f\u548c\u6c22\u53cd\u5e94\uff0c\u5316\u5b66\u53cd\u5e94\u5982\u56fe4\u6240\u793a\u3002<\/p>\n<p><a href=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/6-32.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-32764 \" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/6-32.jpg\" alt=\"\" width=\"640\" height=\"145\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/6-32.jpg 768w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/6-32-300x68.jpg 300w, https:\/\/assets.www.gsbet888.com\/uploads\/2020\/05\/6-32-680x154.jpg 680w\" sizes=\"(max-width: 640px) 100vw, 640px\" \/><\/a><\/p>\n<p style=\"text-align: center;\">\u56fe4. NaOCl\u548cNaNO<sub>3<\/sub>\u6dec\u706d\u96f7\u5c3c\u94b4\u7684\u5316\u5b66\u53cd\u5e94\u5f0f. \u56fe\u7247\u6765\u6e90\uff1a<em>Org. Process Res. Dev.<\/em><\/p>\n<h4>\u603b\u7ed3<\/h4>\n<p>\u901a\u8fc7\u7528NaNO<sub>3<\/sub>\u6c34\u6eb6\u6db2\u6dec\u706d\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\uff0c\u4f5c\u8005\u5efa\u7acb\u4e86\u5b89\u5168\u7684\u540e\u5904\u7406\u65b9\u5f0f\uff0c\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u53ef\u4ee5\u5728\u7a7a\u6c14\u4e2d\u7a33\u5b9a\u653e\u7f6e\uff0c\u4e0d\u4f1a\u6709\u4efb\u4f55\u6c27\u5316\u653e\u70ed\u73b0\u8c61\uff0c\u4ece\u800c\u53ef\u4ee5\u7528\u4e8e\u5927\u89c4\u6a21\u751f\u4ea7\u4e2d\uff0c\u8fdb\u800c\u836f\u7269\u5408\u6210\u4e5f\u53ef\u4ee5\u7528\u96f7\u5c3c\u94b4\u6216\u96f7\u5c3c\u954d\u8fdb\u884c\u8fd8\u539f\u5408\u6210\u3002<\/p>\n<p>\u9644\u5178\u578b\u6dec\u706d\u64cd\u4f5c\uff1a\u96f7\u5c3c\u94b4\uff0835g\uff09\u9996\u5148\u57282-\u7532\u57fa\u56db\u6c22\u544b\u5583\u4e2d\uff08100 mL, ~3.5 vol\uff09\u4e2d\u60ac\u6d6e\uff0c\u7136\u540e\u57284-5barg\u538b\u529b\u7684\u6c22\u6c14\u4e2d\u51b7\u6c34\u6d74\u6e29\u5ea6\u4e0b\u8fd8\u539f1-2\u5c0f\u65f6\u6d3b\u5316\u50ac\u5316\u5242\u3002\u505c\u6b62\u6405\u62cc\u540e\uff0c\u53cd\u5e94\u5668\u7f6e\u6362\u4e3a\u6c2e\u6c14\u3002\u8fc7\u6ee4\u9664\u53bb\u50ac\u5316\u5242\uff0c\u4f9d\u6b21\u7528\u7532\u9187\u6d17\u6da4\uff083 X 100 mL)\uff09\uff0c\u6c34\u6d17\u6da4\uff084 X 100 mL\uff09\u9664\u53bb\u6709\u673a\u76f8\u3002\u6e7f\u6ee4\u997c\u8f6c\u79fb\u81f3RC1\u53cd\u5e94\u91cf\u70ed\u4eea\u4e2d\uff0c\u7528\u6c34\u5206\u6563\uff0c\u8f6c\u901f\u4e3a400RPM\uff0c\u94b4\u50ac\u5316\u5242\u4e3a\u60ac\u6d6e\u6db2\uff0c\u7528\u8ba1\u91cf\u6cf5\u52a0\u516510\u500d\u4f53\u79ef\uff08350ml\uff09\u768410%\u785d\u9178\u94a0\u621610%\u6b21\u6c2f\u9178\u94a0\uff0c\u4f7f\u6700\u7ec8\u6dec\u706d\u6d53\u5ea6\u4e3a5%\u3002\u6bcf\u6b21\u5b9e\u9a8c\u90fd\u76d1\u63a7\u73af\u5883\u6e29\u5ea6\u3002<\/p>\n<h4>\u53c2\u8003\u6587\u732e<\/h4>\n<ul>\n<li>[1] Playing with Fire? A Safe and Effective Deactivation of Raney Cobalt using Aqueous Sodium Nitrate.<\/li>\n<li>[2] John Jin Lim; Frank Dixon, Jr.; David C. Leitch; John Kowalski; Mark Nilson; Charles Goss; Roy Flanagan; Sean Hayes; Michael J. Murphy<\/li>\n<li>[3] Organic Process Research &amp; Development \u00a0ASAP \u00a0DOI: 10.1021\/acs.oprd.0c00053<\/li>\n<\/ul>\n<p>\u672c\u6587\u7248\u6743\u5c5e\u4e8e<strong>\u00a0<a href=\"\/\/www.gsbet888.com\/\">Chem-Station\u5316\u5b66\u7a7a\u95f4<\/a>\uff0c<\/strong>\u00a0\u6b22\u8fce\u70b9\u51fb\u6309\u94ae\u5206\u4eab\uff0c\u672a\u7ecf\u8bb8\u53ef\uff0c\u8c22\u7edd\u8f6c\u8f7d\uff01<\/p>\n","protected":false},"excerpt":{"rendered":"\u672c\u6587\u4f5c\u8005\uff1a\u7af9\u60a0 \u6d77\u7ef5\u72b6\u6216\u591a\u5b54\u91d1\u5c5e\u50ac\u5316\u5242\u96f7\u5c3c\u954dRaney nickel\uff081925\u5e74\u4e13\u5229\uff09\u548c\u96f7\u5c3c\u94b4Raney cobalt\uff081933\u5e74\u4e13\u5229\uff09\uff0c\u5e7f\u6cdb\u5e94\u7528\u5728\u6750\u6599\u548c\u5927\u5b97\u5316\u5b66\u54c1\u5de5\u4e1a\u9886\u57df\u3002\u8fd9\u4e9b\u5ec9\u4ef7\u91d1\u5c5e\uff0c\u5177\u6709\u5f88\u5927\u7684\u6bd4\u8868\u9762\u79ef\uff0c\u56e0\u6b64\u6d3b\u6027\u8f83\u9ad8\uff0c\u800c\u4e14\u591a\u5b54\u7ed3\u6784\u53ef\u4ee5\u5438\u9644\u5927\u91cf\u6c22\u6c14\uff0c\u5728\u6c22\u5316\u53cd\u5e94\u4e2d\u5e94\u7528\u8f83\u591a\u3002\u5c3d\u7ba1\u6709\u79cd\u79cd\u4f18\u70b9\uff0c\u5728\u533b\u836f\u5316\u5de5\u884c\u4e1a\uff0c\u5373\u4f7f\u662f\u5c0f\u89c4\u6a21\u7684\u5b9e\u9a8c\u5ba4\u5408\u6210\uff0c\u4e5f\u5f88\u5c11\u7528\u5230\u5b83\u4eec\uff0c\u4e3b\u8981\u662f\u8fd9\u7c7b\u591a\u5b54\u6750\u6599\u4f1a\u81ea\u71c3\uff0c\u9700\u8981\u683c\u5916\u8003\u8651\u5b89\u5168\u95ee\u9898\u3002\u5373\u4f7f\u50ac\u5316\u5242\u4e3a\u72ec\u7acb\u5305\u88c5\u5bf9\u7a7a\u6c14\u7a33\u5b9a\u7684\u6d46\u72b6\u7269\uff0c\u53cd\u5e94\u7ed3\u675f\u540e\uff0c\u8fc7\u6ee4\u9664\u53bb\u50ac\u5316\u5242\uff0c\u9700\u8981\u7559\u4e00\u90e8\u5206\u6eb6\u5242\u8986\u76d6\u5728\u50ac\u5316\u5242\u8868\u9762\uff0c\u5426\u5219\u62bd\u5e72\u540e\u7684\u96f7\u5c3c\u94b4\u4f1a\u71c3\u70e7\u3002\u800c\u4e14\u6709\u673a\u5316\u5b66\u53cd\u5e94\u4e2d\u7684\u6eb6\u5242\u7edd\u5927\u90e8\u5206\u4e3a\u6709\u673a\u6eb6\u5242\uff0c\u4e5f\u662f\u4e00\u79cd\u6f5c\u5728\u7684\u71c3\u70e7\u7269\uff0c\u5373\u4f7f\u4e0d\u65ad\u5439\u60f0\u6027\u6c14\u4f53\u5982\u6c2e\u6c14\u3001\u6c29\u6c14\u4fdd\u62a4\uff0c\u4e5f\u4e0d\u80fd\u5b8c\u5168\u6d88\u9664\u9690\u60a3\u3002\u56e0\u6b64\u5373\u4f7f\u662f\u5b9e\u9a8c\u5ba4\u5c0f\u89c4\u6a21\u5b9e\u9a8c\uff0c\u4e5f\u4e0d\u80fd\u6389\u4ee5\u8f7b\u5fc3\u3002 \u56fe1 \u82ef\u81481\u7684\u96f7\u5c3c\u94b4\u8fd8\u539f. \u56fe\u7247\u6765\u6e90\uff1aOrg. Process Res. Dev. \u5728\u7814\u7a76\u539f\u6599\u836f\u8fc7\u7a0b\u4e2d\uff0c\u6765\u81ea\u82f1\u56fd\u845b\u5170\u7d20\u53f2\u514bGSK\uff08GlaxoSmithKline\uff09\u7684John Jin Lim\u7b49\uff0c\u5728\u7814\u53d1\u53d6\u4ee3\u7684\u82ef\u81481\u8fd8\u539f\u4e3a\u5bf9\u5e94\u7684\u82c4\u80fa2\u65f6\u3001\u901a\u8fc7\u7b5b\u9009\u548c\u4f18\u5316\u53cd\u5e94\u6761\u4ef6\uff0c\u96f7\u5c3c\u94b4\u662f\u7406\u60f3\u7684\u8fd8\u539f\u5242\uff0c\u53cd\u5e94\u6536\u7387\u9ad8\uff0c\u526f\u4ea7\u7269\u919b3\u3001\u91874\u548c\u4ef2\u80fa5\u90fd\u8f83\u5c11\uff0c\u5982\u56fe1\u6240\u793a\u3002\u5e76\u4e14\u82c4\u80fa2\u4e0d\u7ecf\u7eaf\u5316\u76f4\u63a5\u8fdb\u5165\u4e0b\u4e00\u6b65\u53cd\u5e94\uff0c\u51cf\u5c11\u526f\u4ea7\u7269\u81ea\u7136\u53ef\u63d0\u9ad8\u7ec8\u4ea7\u54c1\u7684\u8d28\u91cf\u3002\u4f46\u96f7\u5c3c\u94b4\u7684\u50ac\u5316\u6548\u679c\u4f4e\u4e8e\u96f7\u5c3c\u954d\u548cPd\/C\u50ac\u5316\u5242\uff0c\u9700\u8981\u589e\u52a0\u6295\u6599\uff0c\u4f18\u5316\u540e\u7684\u7528\u91cf\u4e3a10-20 wt%\u3002\u5de5\u4e1a\u5316\u751f\u4ea7\u8be5\u4ea7\u54c1\u7684\u89c4\u6a21\u9ad8\u8fbe70-100kg\uff0c\u5178\u578b\u7684\u751f\u4ea7\u6279\u91cf\u4e3a\u4ee5100kg\u82ef\u81481\u4e3a\u8d77\u59cb\u7269\u6599\uff0c\u56e0\u6b64\u9700\u898110-20kg\u7684\u96f7\u5c3c\u94b4\uff0c\u5982\u6b64\u5927\u7684\u7528\u91cf\uff0c\u5fc5\u987b\u91cd\u70b9\u8003\u8651\u5b89\u5168\u95ee\u9898\u3002GSK\u7684\u5316\u5b66\u5bb6\u53d1\u73b0\u4e86\u53ef\u4ee5\u5b89\u5168\u5904\u7406\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u7684\u6dec\u706d\u65b9\u6cd5\uff0c\u4f7f\u751f\u4ea7\u66f4\u5b89\u5168\uff0c\u8bba\u6587\u300aPlaying with Fire? A Safe and Effective Deactivation of Raney Cobalt using Aqueous Sodium Nitrate\u300b\u53d1\u8868\u5728\u5de5\u827a\u7814\u53d1\u7684\u8457\u540d\u671f\u520aOrg. Process Res. Dev.\u4e0a\uff0cDOI: 10.1021\/acs.oprd.0c00053. \u5c3d\u7ba1\u96f7\u5c3c\u94b4\u5df2\u7ecf\u53d1\u73b0\u4e86\u8fd1\u767e\u5e74\uff0c\u5173\u4e8e\u5b83\u7684\u7814\u7a76\u62a5\u544a\u5e76\u4e0d\u591a\u3002\u53ef\u4ee5\u786e\u5b9a\u7684\u662f\u96f7\u5c3c\u94b4\u542b\u6709\u6c22\u6c14\uff0c\u867d\u7136\u6bd4\u96f7\u5c3c\u954d\u5c11\uff0c\u4e5f\u8fbe\u523040-70mlH2\/g\u94b4\uff0c\u5e76\u4e14\u7edd\u5927\u90e8\u5206\u6c22\u6c14\u662f\u4e0e\u94b4\u7ed3\u5408\u7684\uff0c\u901a\u8fc7\u62bd\u771f\u7a7a\u53ea\u80fd\u9664\u53bb6%\u7684\u6c22\u6c14\u3002\u96f7\u5c3c\u94b4\u5230\u5e95\u6709\u591a\u5371\u9669\uff0c\u5c1a\u672a\u6709\u7b2c\u4e00\u624b\u8d44\u6599\u3002\u5178\u578b\u7684\u5b9e\u9a8c\u5ba4\u89c4\u6a21\u7684\u6c22\u5316\u53cd\u5e94\u4e2d\uff0c\u5c061g\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u5206\u79bb\u51fa\u6765\u540e\uff0c\u5728\u73bb\u7483\u6f0f\u6597\u4e2d\u62bd\u6ee4\u5e72\u71e5\uff0c\u5e76\u76d1\u63a7\u6e29\u5ea6\u3002\u5e72\u71e5\u540e2-3\u79d2\uff0c\u7a81\u7136\u653e\u70ed\uff0c\u6e29\u5ea6\u98d9\u5347\u81f3350\u2103\uff08\u76d1\u6d4b\u5668\u7684\u6781\u9650\uff09\uff0c\u5e76\u53d1\u51fa\u70bd\u70ed\uff0c\u8bf4\u660e\u6e29\u5ea6\u81f3\u5c11\u4e3a525\u2103\uff0c\u5982\u56fe2\u6240\u793a\u3002\u5f88\u660e\u663e\uff0c\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u5177\u6709\u5371\u9669\u6027\uff0c\u5c3d\u7ba1\u6709\u62a5\u9053\u5b83\u4e0d\u5982\u96f7\u5c3c\u954d\uff0c\u6240\u4ee5\u5728\u4f7f\u7528\u96f7\u5c3c\u94b4\u65f6\u4e0d\u80fd\u62bd\u5e72\uff0c\u9700\u8981\u8986\u76d6\u4e00\u5c42\u6eb6\u5242\u6216\u6c34\u9632\u6b62\u71c3\u70e7\u3002\u5982\u679c\u627e\u4e0d\u5230\u5408\u9002\u7684\u96f7\u5c3c\u94b4\u540e\u5904\u7406\u65b9\u6cd5\uff0c\u96be\u4ee5\u83b7\u5f97\u5b89\u5168\u7684\u751f\u4ea7\u5de5\u827a\uff0c\u6240\u4ee5\u4f5c\u8005\u5fc5\u987b\u626b\u9664\u8fd9\u4e2a\u969c\u788d\u3002 \u56fe2. \u76d1\u63a7\u62bd\u6ee4\u8fc7\u7a0b\u4e2d\u96f7\u5c3c\u94b4\u7684\u6e29\u5ea6\u548c\u653e\u70ed\u73b0\u8c61. \u56fe\u7247\u6765\u6e90\uff1aOrg. Process Res. Dev. \u5bf9\u6b64\uff0c\u4f5c\u8005\u8bc4\u4f30\u4e86\u4e0d\u540c\u7684\u6dec\u706d\u65b9\u6cd5\u53ca\u4f34\u751f\u7684\u5371\u9669\u3002\u5b9e\u9a8c\u5ba4\u5e38\u7528\u7684\u65b9\u6cd5\u4e3a\u52a0\u5165\u65e0\u673a\u9178\u5982\u76d0\u9178\uff0c\u4f46\u540c\u6837\u4f1a\u5267\u70c8\u653e\u70ed\u91ca\u653e\u6c22\u6c14\u3002\u800c\u4e14\u8981\u4ece\u62bd\u6ee4\u88c5\u7f6e\u4e2d\u8f6c\u79fb\u5230\u6dec\u706d\u88c5\u7f6e\u4e2d\uff0c\u8fc7\u7a0b\u540c\u6837\u6709\u5371\u9669\u3002\u4f7f\u7528\u8fc7\u7684\u6d77\u7ef5\u72b6\u50ac\u5316\u5242\u4ea7\u751f\u5316\u5b66\u5371\u9669\u7684\u6839\u6e90\u662f\u8868\u9762\u4e0a\u7684\u6d3b\u6027\u6c22\u6216\u8005\u7a7a\u4f4d\u53ef\u4ee5\u548c\u6c27\u6c14\u53cd\u5e76\u653e\u70ed\u3002\u56e0\u6b64\u4f5c\u8005\u8003\u8651\u53e6\u4e00\u79cd\u7b56\u7565\uff0c\u7528\u6c27\u5316\u5242\u5e76\u63a7\u5236\u6c27\u5316\u901f\u7387\u4ee5\u63a7\u5236\u653e\u70ed\uff0c\u5e76\u63a7\u5236\u5347\u6e29\u4e0d\u8d85\u8fc720\u2103\u3002 \u5bf9\u4e8e\u96f7\u5c3c\u954d\uff0c\u53ef\u4ee5\u75288:1 v\/w\u76845%\u6b21\u6c2f\u9178\u94a0\u6eb6\u6db2\uff08\u6f02\u767d\u5242\uff09\u5904\u7406\uff0c\u4f46\u53ef\u80fd\u4e0d\u9002\u7528\u4e8e\u96f7\u5c3c\u94b4\uff0c\u6b21\u6c2f\u9178\u94a0NaOCl\u4f1a\u91ca\u653e\u6c27\u6c14\u5f15\u53d1\u53e6\u5916\u7684\u5371\u9669\u3002\u53d7\u52301957\u5e74\u675c\u90a6DuPont\u4e00\u7bc7\u7528\u785d\u9178\u94a0\uff08NaNO3\uff09\u6405\u62cc30min\u6dec\u706d\u96f7\u5c3c\u954d\u7684\u4e13\u5229\u542f\u53d1\uff0c\u4f5c\u8005\u5c1d\u8bd5\u7528\u785d\u9178\u94a0\u3001\u4e9a\u785d\u9178\u94a0\u6eb6\u6db2\u6dec\u706d\u96f7\u5c3c\u94b4\uff0c\u4f46\u4e9a\u785d\u9178\u94a0\u7684\u6548\u7387\u8f83\u5dee\u3002 \u88681. NaNO3\u548cNaOCl\u6dec\u706d\u7684\u653e\u70ed \u4e3a\u6bd4\u8f83\u4e24\u79cd\u6c27\u5316\u5242\u7684\u6dec\u706d\u6548\u679c\uff0c\u4f5c\u8005\u7528\u91cf\u70ed\u6cd5\u6bd4\u8f83NaNO3\u548cNaOCl\u5206\u522b\u5904\u740635g\u96f7\u5c3c\u94b4\uff08\u89c1\u5178\u578b\u6dec\u706d\u64cd\u4f5c\uff09\uff0c\u4f7f\u7528\u91cf\u4e3a20:1 v\/w\u4ee5\u5145\u5206\u6dec\u706d\u548c\u51b7\u5374\u653e\u51fa\u7684\u70ed\u91cf\u3002\u540c\u65f6\u7528CHETAH\u8ba1\u7b97\u7406\u8bba\u653e\u70ed\u91cf\u548c\u76d1\u63a7\u5b9e\u9645\u653e\u70ed\u91cf\uff0c\u4e24\u8005\u51e0\u4e4e\u4e00\u6837\uff0c\u7ed3\u679c\u89c1\u88681\u6570\u636e\u6240\u793a\u3002\u4e24\u79cd\u6c27\u5316\u5242\u90fd\u53ef\u4ee5\u6dec\u706d\u96f7\u5c3c\u94b4\uff0c\u62bd\u6ee4\u5e72\u71e5\u540e\uff0c\u5373\u4f7f\u7528\u52a0\u70ed\u677f\u5e72\u71e5\uff0c\u4e5f\u6ca1\u6709\u53d1\u73b0\u653e\u70ed\u73b0\u8c61\u3002NaNO3\u4f18\u52bf\u66f4\u660e\u663e\uff0c\u4f53\u7cfb\u6e29\u5ea6\u53ea\u4e0a\u5347\u4e8612\u2103\uff0c\u4f4e\u4e8e20\u2103\u7684\u9884\u671f\u5b89\u5168\u9650\u5ea6\uff0c\u800c\u4e14NaNO3\u4f1a\u91ca\u653e\u6c2e\u6c14\uff0cNaOCl\u91ca\u653e\u6c27\u6c14\u548c\u5c11\u91cf\u6c2e\u6c14\uff0c\u5982\u56fe3\u6240\u793a\u3002 \u56fe3. \u76d1\u63a7\u6dec\u706d\u8fc7\u7a0b\u4e2d\u7684\u6e29\u5ea6\u548c\u6c14\u4f53\u653e\u51fa\u60c5\u51b5\u3002\u56fe\u7247\u6765\u6e90\uff1aOrg. Process Res. Dev. \u800c\u4e14NaOCl\u548cNaNO3\u6dec\u706d\u96f7\u5c3c\u94b4\uff0c\u4e3b\u8981\u662f\u548c\u6c22\u53cd\u5e94\uff0c\u5316\u5b66\u53cd\u5e94\u5982\u56fe4\u6240\u793a\u3002 \u56fe4. NaOCl\u548cNaNO3\u6dec\u706d\u96f7\u5c3c\u94b4\u7684\u5316\u5b66\u53cd\u5e94\u5f0f. \u56fe\u7247\u6765\u6e90\uff1aOrg. Process Res. Dev. \u603b\u7ed3 \u901a\u8fc7\u7528NaNO3\u6c34\u6eb6\u6db2\u6dec\u706d\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\uff0c\u4f5c\u8005\u5efa\u7acb\u4e86\u5b89\u5168\u7684\u540e\u5904\u7406\u65b9\u5f0f\uff0c\u4f7f\u7528\u8fc7\u7684\u96f7\u5c3c\u94b4\u53ef\u4ee5\u5728\u7a7a\u6c14\u4e2d\u7a33\u5b9a\u653e\u7f6e\uff0c\u4e0d\u4f1a\u6709\u4efb\u4f55\u6c27\u5316\u653e\u70ed\u73b0\u8c61\uff0c\u4ece\u800c\u53ef\u4ee5\u7528\u4e8e\u5927\u89c4\u6a21\u751f\u4ea7\u4e2d\uff0c\u8fdb\u800c\u836f\u7269\u5408\u6210\u4e5f\u53ef\u4ee5\u7528\u96f7\u5c3c\u94b4\u6216\u96f7\u5c3c\u954d\u8fdb\u884c\u8fd8\u539f\u5408\u6210\u3002 \u9644\u5178\u578b\u6dec\u706d\u64cd\u4f5c\uff1a\u96f7\u5c3c\u94b4\uff0835g\uff09\u9996\u5148\u57282-\u7532\u57fa\u56db\u6c22\u544b\u5583\u4e2d\uff08100 mL, ~3.5 vol\uff09\u4e2d\u60ac\u6d6e\uff0c\u7136\u540e\u57284-5barg\u538b\u529b\u7684\u6c22\u6c14\u4e2d\u51b7\u6c34\u6d74\u6e29\u5ea6\u4e0b\u8fd8\u539f1-2\u5c0f\u65f6\u6d3b\u5316\u50ac\u5316\u5242\u3002\u505c\u6b62\u6405\u62cc\u540e\uff0c\u53cd\u5e94\u5668\u7f6e\u6362\u4e3a\u6c2e\u6c14\u3002\u8fc7\u6ee4\u9664\u53bb\u50ac\u5316\u5242\uff0c\u4f9d\u6b21\u7528\u7532\u9187\u6d17\u6da4\uff083 X 100 mL)\uff09\uff0c\u6c34\u6d17\u6da4\uff084 X 100 mL\uff09\u9664\u53bb\u6709\u673a\u76f8\u3002\u6e7f\u6ee4\u997c\u8f6c\u79fb\u81f3RC1\u53cd\u5e94\u91cf\u70ed\u4eea\u4e2d\uff0c\u7528\u6c34\u5206\u6563\uff0c\u8f6c\u901f\u4e3a400RPM\uff0c\u94b4\u50ac\u5316\u5242\u4e3a\u60ac\u6d6e\u6db2\uff0c\u7528\u8ba1\u91cf\u6cf5\u52a0\u516510\u500d\u4f53\u79ef\uff08350ml\uff09\u768410%\u785d\u9178\u94a0\u621610%\u6b21\u6c2f\u9178\u94a0\uff0c\u4f7f\u6700\u7ec8\u6dec\u706d\u6d53\u5ea6\u4e3a5%\u3002\u6bcf\u6b21\u5b9e\u9a8c\u90fd\u76d1\u63a7\u73af\u5883\u6e29\u5ea6\u3002 \u53c2\u8003\u6587\u732e [1] Playing with Fire? A Safe and Effective Deactivation of Raney Cobalt using Aqueous Sodium Nitrate. [2] John Jin Lim; Frank Dixon, Jr.; David C. Leitch; John Kowalski; Mark Nilson; Charles Goss; Roy Flanagan; Sean Hayes; Michael J. 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