{"id":49380,"date":"2024-04-02T08:00:09","date_gmt":"2024-04-02T00:00:09","guid":{"rendered":"\/\/www.gsbet888.com\/?p=49380"},"modified":"2024-04-01T10:20:21","modified_gmt":"2024-04-01T02:20:21","slug":"%e3%80%8cspotlight-research%e3%80%8d%e9%95%8d%e5%82%ac%e5%8c%96%e7%9a%84%e8%bd%b4%e5%90%91%e9%80%89%e6%8b%a9%e6%80%a7c-h%e7%83%b7%e5%9f%ba%e5%8c%96","status":"publish","type":"post","link":"\/\/www.gsbet888.com\/%e5%8c%96%e5%ad%a6%e6%9d%82%e8%ae%b0\/recentpaper\/%e7%83%ad%e7%82%b9%e7%a0%94%e7%a9%b6\/2024\/04\/%e3%80%8cspotlight-research%e3%80%8d%e9%95%8d%e5%82%ac%e5%8c%96%e7%9a%84%e8%bd%b4%e5%90%91%e9%80%89%e6%8b%a9%e6%80%a7c-h%e7%83%b7%e5%9f%ba%e5%8c%96.html","title":{"rendered":"\u300cSpotlight Research\u300d\u954d\u50ac\u5316\u7684\u8f74\u5411\u9009\u62e9\u6027C\u2013H\u70f7\u57fa\u5316"},"content":{"rendered":"<p style=\"text-align: justify;\"><strong>\u4f5c\u8005\uff1a<\/strong><strong>\u77f3\u6cb9\u919a<\/strong><\/p>\n<p style=\"text-align: justify;\">\u672c\u671f\u70ed\u70b9\u7814\u7a76\uff0c\u6211\u4eec\u9080\u8bf7\u5230\u4e86\u672c\u6587\u7b2c\u4e00\u4f5c\u8005\u6765\u81ea\u54e5\u5ef7\u6839\u5927\u5b66\u7684\u5f20\u5b50\u7af6\u535a\u58eb\u4e3a\u6211\u4eec\u5206\u4eab\u3002<\/p>\n<p style=\"text-align: justify;\">2024\u5e743\u670821\u65e5\uff0c<em>J. Am. Chem. Soc.<\/em>\u5728\u7ebf\u53d1\u8868\u4e86\u6765\u81ea<strong>\u54e5\u5ef7\u6839\u5927\u5b66<\/strong><strong>Lutz Ackermann<\/strong><strong>\u6559\u6388<\/strong>\u56e2\u961f\u9898\u4e3a\u300cNickel-Catalyzed Atroposelective C\u2013H Alkylation Enabled by Bimetallic Catalysis with Air-Stable Heteroatom-Substituted Secondary Phosphine Oxide Preligands\u300d\u7684\u7814\u7a76\u8bba\u6587\u3002\u4f5c\u8005\u62a5\u9053\u4e86\u7b2c\u4e00\u4f8b\u954d\u50ac\u5316\u7684\u8f74\u5411\u9009\u62e9\u6027C\u2013H\u70f7\u57fa\u5316\u53cd\u5e94\uff0c\u901a\u8fc7\u4f7f\u7528\u65b0\u578b\u624b\u6027\u6742\u539f\u5b50\u53d6\u4ee3\u7684\u4ef2\u6c27\u5316\u81a6\uff08HASPO\uff09\u914d\u4f4d\u7684Ni-Al\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u5b9e\u73b0\u4e86\u591a\u79cd\u5177\u6709C\u2013N\u8f74\u624b\u6027\u7684\u82ef\u5e76\u54aa\u5511\u884d\u751f\u7269\u7684\u5408\u6210\u3002\u6b64\u5916\uff0cDFT\u8ba1\u7b97\u548c\u6570\u636e\u79d1\u5b66\u5206\u6790\u63ed\u793a\u4e86\u50ac\u5316\u5242\u7684\u4f5c\u7528\u6a21\u5f0f\uff0c\u5e76\u9610\u660e\u4e86\u8d1f\u8d23\u63a7\u5236\u5bf9\u6620\u9009\u62e9\u6027\u7684\u624b\u6027\u9884\u914d\u4f53\u7684\u5173\u952e\u7279\u5f81\u3002<\/p>\n<p style=\"text-align: justify;\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-49382 size-full\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image002.jpg\" alt=\"\" width=\"627\" height=\"287\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image002.jpg 627w, https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image002-300x137.jpg 300w, https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image002-370x170.jpg 370w\" sizes=\"(max-width: 627px) 100vw, 627px\" \/><\/p>\n<blockquote>\n<p style=\"text-align: justify;\">\u201cNickel-Catalyzed Atroposelective C\u2013H Alkylation Enabled by Bimetallic Catalysis with Air-Stable Heteroatom-Substituted Secondary Phosphine Oxide Preligands<\/p>\n<p style=\"text-align: justify;\">Zi-Jing Zhang, Matthias M. Simon, Shuang Yu, Shu-Wen Li, Xinran Chen, Silvia Cattani, Xin Hong*, and Lutz Ackermann*<\/p>\n<p style=\"text-align: justify;\"><em>J. Am. Chem. Soc.<\/em><strong> 2024<\/strong><em>.<\/em> doi: <a href=\"https:\/\/doi.org\/10.1021\/jacs.3c14600\">10.1021\/jacs.3c14600<\/a>\u201d<\/p>\n<\/blockquote>\n<h4 style=\"text-align: justify;\"><strong>Q1. <\/strong><strong>\u8bf7\u5bf9\u201c<\/strong><strong>Nickel-Catalyzed Atroposelective C\u2013H Alkylation Enabled by Bimetallic Catalysis with Air-Stable Heteroatom-Substituted Secondary Phosphine Oxide Preligands<\/strong><strong>\u201d<\/strong><strong>\u4f5c<\/strong><strong>\u4e00\u4e2a\u7b80\u5355\u4ecb\u7ecd\u3002<\/strong><\/h4>\n<p style=\"text-align: justify;\">C\u2013N\u8f74\u624b\u6027\u5316\u5408\u7269\u5e7f\u6cdb\u5b58\u5728\u4e8e\u5929\u7136\u4ea7\u7269\u548c\u836f\u7269\u5206\u5b50\u4e2d\uff0c\u4f46\u7531\u4e8e\u65cb\u8f6c\u80fd\u5792\u8f83\u4f4e\uff0c\u5176\u50ac\u5316\u4e0d\u5bf9\u79f0\u5408\u6210\u4ecd\u7136\u662f\u5177\u6709\u6311\u6218\u6027\u7684\u5de5\u4f5c\u3002\u76ee\u524dC\u2014N\u8f74\u624b\u6027\u5316\u5408\u7269\u7684\u4e0d\u5bf9\u79f0\u5408\u6210\u5f88\u5927\u7a0b\u5ea6\u4e0a\u4f9d\u8d56\u4e8e\u6bd2\u6027\u8f83\u5927\u4e14\u4ef7\u683c\u6602\u8d35\u76844d\u30015d\u8fc7\u6e21\u91d1\u5c5e\u50ac\u5316\u5242\uff0c\u4f7f\u7528\u5ec9\u4ef73d\u91d1\u5c5e\u50ac\u5316\u5242\u7684\u62a5\u9053\u8fd8\u5f88\u7f3a\u4e4f\u3002\u5728\u672c\u6587\u4e2d\u6211\u4eec\u62a5\u9053\u4e86\u7b2c\u4e00\u4f8b\u954d\u50ac\u5316\u7684\u8f74\u5411\u9009\u62e9\u6027C\u2013H\u70f7\u57fa\u5316\u53cd\u5e94\uff0c\u901a\u8fc7\u4f7f\u7528\u65b0\u578b\u624b\u6027\u6742\u539f\u5b50\u53d6\u4ee3\u7684\u4ef2\u6c27\u5316\u81a6\uff08HASPO\uff09\u914d\u4f4d\u7684Ni-Al\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u5b9e\u73b0\u4e86\u591a\u79cd\u5177\u6709C\u2013N\u8f74\u624b\u6027\u7684\u82ef\u5e76\u54aa\u5511\u884d\u751f\u7269\u7684\u5408\u6210 \u3002\u8be5\u53cd\u5e94\u4e0e\u5305\u542b\u82b3\u57fa\u70ef\u70c3\u3001\u70f7\u57fa\u70ef\u70c3\u3001\u5185\u70ef\u70c3\u30011,3-\u4e8c\u70ef\u5728\u5185\u7684\u591a\u79cd\u70ef\u70c3\u5177\u6709\u826f\u597d\u7684\u76f8\u5bb9\u6027\u3002\u6b64\u5916\u6211\u4eec\u8fd8\u901a\u8fc7DFT\u8ba1\u7b97\u548c\u6570\u636e\u79d1\u5b66\u5206\u6790\u63ed\u793a\u4e86\u50ac\u5316\u5242\u7684\u4f5c\u7528\u6a21\u5f0f\uff0c\u5e76\u9610\u660e\u4e86\u8d1f\u8d23\u63a7\u5236\u5bf9\u6620\u9009\u62e9\u6027\u7684\u624b\u6027\u9884\u914d\u4f53\u7684\u5173\u952e\u7279\u5f81\u3002<\/p>\n<h4 style=\"text-align: justify;\"><strong>Q2. <\/strong><strong>\u6709\u5173\u672c\u6b21\u7814\u7a76\u7684\u65f6\u5019\u9047\u5230\u8fc7\u600e\u6837\u7684\u56f0\u96be\u5462\uff1f\u53c8\u662f\u600e\u6837\u514b\u670d\u7684\u5462<\/strong><\/h4>\n<p style=\"text-align: justify;\">\u5728\u6b64\u5de5\u4f5c\u4e2d\u9047\u5230\u7684\u56f0\u96be\u4e3b\u8981\u662f\u5728\u624b\u6027\u914d\u4f53\u7684\u8bbe\u8ba1\u65b9\u9762\uff0c\u6211\u4eec\u53d1\u73b0\u4f7f\u7528C2\u975e\u5bf9\u79f0\u7684\u624b\u6027\u4e8c\u80fa\u884d\u751f\u7684HASPO\u9884\u914d\u4f53\u53ef\u4ee5\u5b9e\u73b0\u53cd\u5e94\u7acb\u4f53\u9009\u62e9\u6027\u7684\u521d\u6b65\u63a7\u5236\uff0c\u4f46\u662f\u96be\u4ee5\u83b7\u5f97\u5f88\u9ad8\u7684\u5bf9\u6620\u9009\u62e9\u6027\u3002\u540e\u6765\u6211\u4eec\u901a\u8fc7\u5728\u624b\u6027\u9884\u914d\u4f53\u82b3\u73af\u4e0d\u540c\u4f4d\u7f6e\u5f15\u5165\u591a\u6837\u5316\u7684\u53d6\u4ee3\u57fa\uff0c\u6539\u53d8\u4e86\u624b\u6027\u9884\u914d\u4f53\u7684\u7a7a\u95f4\u7ed3\u6784\u548c\u7535\u6027\uff0c\u6700\u7ec8\u5b9e\u73b0\u4e86\u53cd\u5e94\u7684\u9ad8\u7acb\u4f53\u9009\u62e9\u6027\u63a7\u5236\u3002<\/p>\n<h4 style=\"text-align: justify;\"><strong>Q3. <\/strong><strong>\u672c\u6b21\u7814\u7a76\u4e3b\u4f53\uff0c\u6709\u6ca1\u6709\u4ec0\u4e48\u8ba9\u60a8\u611f\u89c9\u7279\u522b\u8f9b\u82e6\u548c\u70e7\u8111\u5462\uff1f<\/strong><\/h4>\n<p style=\"text-align: justify;\">\u624b\u6027HASPO\u9884\u914d\u4f53\u7684\u8bbe\u8ba1\u5408\u6210\u662f\u975e\u5e38\u7e41\u7410\u548c\u8f9b\u82e6\u7684\u5de5\u4f5c\u3002\u4e3a\u4e86\u4e86\u89e3\u624b\u6027\u9884\u914d\u4f53\u7684\u7ed3\u6784\u5bf9\u53cd\u5e94\u7acb\u4f53\u9009\u62e9\u6027\u7684\u5f71\u54cd\uff0c\u6211\u4eec\u901a\u8fc7\u6570\u636e\u79d1\u5b66\u5206\u6790\u8fdb\u4e00\u6b65\u89e3\u6790\u4e86\u624b\u6027\u9884\u914d\u4f53\u7684\u5173\u952e\u7279\u5f81\u3002<\/p>\n<h4 style=\"text-align: justify;\"><strong>Q4. <\/strong><strong>\u5c06\u6765\u60f3\u7ee7\u7eed\u7814\u7a76\u5316\u5b66\u7684\u54ea\u4e2a\u65b9\u5411\u5462\uff1f<\/strong><\/h4>\n<p style=\"text-align: justify;\">\u6211\u4eec\u63a5\u4e0b\u6765\u8fd8\u5c06\u4e13\u6ce8\u4e8e\u4f7f\u7528\u5ec9\u4ef7\u91d1\u5c5e\u5b9e\u73b0\u591a\u79cd\u6709\u4ef7\u503c\u7684\u4e0d\u5bf9\u79f0\u50ac\u5316\u53cd\u5e94\u3002<\/p>\n<h4 style=\"text-align: justify;\"><strong>Q5. <\/strong><strong>\u6700\u540e\uff0c\u6709\u4ec0\u4e48\u60f3\u5bf9\u5404\u4f4d\u8bfb\u8005\u8bf4\u7684\u5417\uff1f<\/strong><\/h4>\n<p style=\"text-align: justify;\">\u5e0c\u671b\u5927\u5bb6\u4f1a\u559c\u6b22\u672c\u6587\u7684\u5de5\u4f5c\u3002\u9884\u795d\u5404\u4f4d\u540c\u884c\u8eab\u4f53\u5065\u5eb7\u3001\u5de5\u4f5c\u987a\u5229\u3002<\/p>\n<h4 style=\"text-align: justify;\"><strong>\u4f5c\u8005\u6559\u80b2\u80cc\u666f\u7b80\u4ecb<\/strong><\/h4>\n<p style=\"text-align: justify;\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-49383 size-full\" src=\"https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image003-1.jpg\" alt=\"\" width=\"415\" height=\"311\" srcset=\"https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image003-1.jpg 415w, https:\/\/assets.www.gsbet888.com\/uploads\/2024\/04\/image003-1-300x225.jpg 300w\" sizes=\"(max-width: 415px) 100vw, 415px\" \/><\/p>\n<p style=\"text-align: justify;\"><strong>\u6559\u80b2\u80cc\u666f\uff1a<\/strong><\/p>\n<p style=\"text-align: justify;\">2012.09-2016.06 \u5170\u5dde\u5927\u5b66\uff0c\u5316\u5b66\u57fa\u5730\u73ed\uff0c\u7406\u5b66\u5b66\u58eb<\/p>\n<p style=\"text-align: justify;\">2016.09-2021.06 \u4e2d\u56fd\u79d1\u5b66\u6280\u672f\u5927\u5b66\uff0c\u6709\u673a\u5316\u5b66\uff0c\u7406\u5b66\u535a\u58eb<\/p>\n<p style=\"text-align: justify;\">2021.08-\u81f3\u4eca \u54e5\u5ef7\u6839\u5927\u5b66\uff0c\u6d2a\u5821\u5b66\u8005\uff0c\u535a\u58eb\u540e<\/p>\n<p style=\"text-align: justify;\"><strong>\u83b7\u5f97\u5956\u52b1\uff1a<\/strong><\/p>\n<p style=\"text-align: justify;\">2018\u5e74\u7814\u7a76\u751f\u56fd\u5bb6\u5956\u5b66\u91d1<\/p>\n<p style=\"text-align: justify;\">2020\u5e74\u7814\u7a76\u751f\u56fd\u5bb6\u5956\u5b66\u91d1<\/p>\n<p style=\"text-align: justify;\">2021\u5e74\u5b89\u5fbd\u7701\u4f18\u79c0\u6bd5\u4e1a\u751f<\/p>\n<p style=\"text-align: justify;\">2021\u5e74\u4e2d\u79d1\u9662\u9662\u957f\u4f18\u79c0\u5956<\/p>\n<p style=\"text-align: justify;\">2022\u5e74\u5fb7\u56fd\u6d2a\u5821\u535a\u58eb\u540e\u5956\u5b66\u91d1<\/p>\n<p style=\"text-align: justify;\">\u672c\u6587\u7248\u6743\u5c5e\u4e8e\u00a0Chem-Station\u5316\u5b66\u7a7a\u95f4\uff0c \u6b22\u8fce\u70b9\u51fb\u6309\u94ae\u5206\u4eab\uff0c\u672a\u7ecf\u8bb8\u53ef\uff0c\u8c22\u7edd\u8f6c\u8f7d.<\/p>\n","protected":false},"excerpt":{"rendered":"\u4f5c\u8005\uff1a\u77f3\u6cb9\u919a \u672c\u671f\u70ed\u70b9\u7814\u7a76\uff0c\u6211\u4eec\u9080\u8bf7\u5230\u4e86\u672c\u6587\u7b2c\u4e00\u4f5c\u8005\u6765\u81ea\u54e5\u5ef7\u6839\u5927\u5b66\u7684\u5f20\u5b50\u7af6\u535a\u58eb\u4e3a\u6211\u4eec\u5206\u4eab\u3002 2024\u5e743\u670821\u65e5\uff0cJ. Am. Chem. Soc.\u5728\u7ebf\u53d1\u8868\u4e86\u6765\u81ea\u54e5\u5ef7\u6839\u5927\u5b66Lutz Ackermann\u6559\u6388\u56e2\u961f\u9898\u4e3a\u300cNickel-Catalyzed Atroposelective C\u2013H Alkylation Enabled by Bimetallic Catalysis with Air-Stable Heteroatom-Substituted Secondary Phosphine Oxide Preligands\u300d\u7684\u7814\u7a76\u8bba\u6587\u3002\u4f5c\u8005\u62a5\u9053\u4e86\u7b2c\u4e00\u4f8b\u954d\u50ac\u5316\u7684\u8f74\u5411\u9009\u62e9\u6027C\u2013H\u70f7\u57fa\u5316\u53cd\u5e94\uff0c\u901a\u8fc7\u4f7f\u7528\u65b0\u578b\u624b\u6027\u6742\u539f\u5b50\u53d6\u4ee3\u7684\u4ef2\u6c27\u5316\u81a6\uff08HASPO\uff09\u914d\u4f4d\u7684Ni-Al\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u5b9e\u73b0\u4e86\u591a\u79cd\u5177\u6709C\u2013N\u8f74\u624b\u6027\u7684\u82ef\u5e76\u54aa\u5511\u884d\u751f\u7269\u7684\u5408\u6210\u3002\u6b64\u5916\uff0cDFT\u8ba1\u7b97\u548c\u6570\u636e\u79d1\u5b66\u5206\u6790\u63ed\u793a\u4e86\u50ac\u5316\u5242\u7684\u4f5c\u7528\u6a21\u5f0f\uff0c\u5e76\u9610\u660e\u4e86\u8d1f\u8d23\u63a7\u5236\u5bf9\u6620\u9009\u62e9\u6027\u7684\u624b\u6027\u9884\u914d\u4f53\u7684\u5173\u952e\u7279\u5f81\u3002 \u201cNickel-Catalyzed Atroposelective C\u2013H Alkylation Enabled by Bimetallic Catalysis with Air-Stable Heteroatom-Substituted Secondary Phosphine Oxide Preligands Zi-Jing Zhang, Matthias M. Simon, Shuang Yu, Shu-Wen Li, Xinran Chen, Silvia Cattani, Xin Hong*, and Lutz Ackermann* J. Am. Chem. Soc. 2024. doi: 10.1021\/jacs.3c14600\u201d Q1. \u8bf7\u5bf9\u201cNickel-Catalyzed Atroposelective C\u2013H Alkylation Enabled by Bimetallic Catalysis with Air-Stable Heteroatom-Substituted Secondary Phosphine Oxide Preligands\u201d\u4f5c\u4e00\u4e2a\u7b80\u5355\u4ecb\u7ecd\u3002 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